Spectroscopy App Note:
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June 2015 
 

 
Analysis of Stainless Steel by Dual View Inductively Coupled Plasma Spectrometry
This application note will demonstrate the ability of High Dispersion ICP-OES in the determination of alloying elements in stainless steels. The dual viewing capability will be used to determine the high concentration elements on the radial view while the axial view will determine the lower concentration, such as phosphorus (P) and sulfur (S). Stainless steels are a corrosion-resistant family of iron alloys. The corrosion resistance is due to the formation of a passive chromium (III) oxide (Cr2O3) layer on the surface of the steel. If this layer is damaged by cutting, scratching or abrasion, it will regenerate, provided sufficient oxygen is available, preventing corrosion. Stainless steels have poor corrosion resistance in low oxygen environments since the oxide layer cannot be repaired quickly enough.
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WDXRF Fused Bead Analysis of Various Oxides
This application note demonstrates that single calibration for diverse materials, such as minerals, ores, and refractories, was established by the fusion method on the Rigaku Supermini200, a benchtop WDXRF spectrometer.
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ICP Analysis of Elemental Impurities in Accordance with the ICH Q3D Guideline
In the ICH Q3D Guideline for Elemental Impurities, 24 elemental impurities were identified as elements of concern due to their toxicity, and permitted daily exposure limits (PDE) were established. This application note presents a quick, accurate analysis of these elements.
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Stainless Steel Analysis Using Handheld LIBS with FLASH Lasing Technology
Analysis of stainless steels and nickel alloys with handheld LIBS has proven challenging because Molybdenum – a key alloy element in the 0.5-3% level – is refractory and requires a much hotter plasma than many miniature, commercially available lasers can provide. A new proprietary laser design was utilized in a handheld LIBS analyzer and is shown to provide much better quantitative analysis of Mo down to 0.15% concentration.
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Miniature 60 kV, 1000 µA 12W X-ray Source
Moxtek's MAGPRO miniature x-ray source which is capable of up to 60 kV 200 µA and down to 4 kV and 1000 µA, and limited to an output power of 12 Watts. The 12W source is meant for use in small beach top systems where small size is valued.
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