Spectroscopy App Note:
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July 2014 

 
Mercury Detection in Nutraceutical Products by Thermal Decomposition
Sumedh Phatak, Milestone Inc.
With the nutraceutical market’s expansion, heavy metals testing has gained tremendous attention. Direct mercury analysis is a fast, cost-effect alternative to time-consuming, labor-intensive techniques like CVAA and ICP-MS for mercury analysis in nutraceuticals.
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Increase Sample Throughput on a CVAA Mercury Analyzer
James Block, Jeff Forsberg, and Matt Nigro, Teledyne CETAC Technologies
In this study, we utilize the CETAC QuickTrace™ M-7600 Cold Vapor Atomic Absorbance Analyzer in conjunction with the ASXPRESS® PLUS to increase throughput while maintaining low detection limits.
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Ultra-Fast Determination of Trace Elements in Water, Conforming to US EPA 200.7 Using the Agilent 5100 Synchronous Vertical Dual View ICP-OES
John Cauduro and Andrew Ryan, Agilent Technologies
The Agilent 5100 Synchronous Vertical Dual View (SVDV) ICP-OES, combined with an SPS 3 autosampler and the SVS 2+ switching valve is an ideal instrument to the meet the productivity demands of environmental labs working to EPA methodology such as 200.7. The instrumentation achieves an excellent sample-to-sample cycle time of 58 s. This enables more samples to be measured each day and reduces argon consumption per sample by 50%.
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Simultaneous Detection of Surface and Bulk Composition of a Magnesium Alloy
Forrest Weesner, TSI Incorporated
In this note, we examine a magnesium alloy plate to determine the type of anti‐corrosion coating present. In the same experiment, the chemistry of the bulk magnesium alloy can also be observed. All data was collected using the ChemReveal® Desktop LIBS Analyzer.
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EDXRF Analysis for Gold Processing
Applied Rigaku Technologies
Cyanide is commonly used to recover gold from gold-bearing ores. Rigaku application note #1299 describes the analysis of gold during leaching, including complete information regarding sample preparation, method calibration, and repeatability.  The results show outstanding performance by the Rigaku NEX QC+ EDXRF analyzer for measuring gold content in aqueous solutions during the processing of gold from ores, tailings, or slags.
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FT-NIR Analysis of Feed Ingredients
Dagmar Behmer, Bruker Optics
Bruker offers the most comprehensive range of FT-NIR solutions for quality control and formulation adjustments with ready to use calibration packages.  Samples can be analyzed nondestructively in seconds, saving cost by reducing time in reagent use.
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Non-Destructive Evaluation of Composite Thermal Damage with Agilent’s New Handheld 4300 Handheld FTIR
Frank Higgins, Agilent Technologies
The increasing use of composites to replace metal components demands more sophisticated diagnostic tools to detect problem and confirm chemical composition of the material. In this application note, we demonstrate that the 4300 Handheld FTIR is an ideal tool for the task, allowing users to effectively measure thermal overexposure and damage in carbon fiber composites at-site without destroying the sample.
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Raman Spectroscopic Detection of Olive Oil Adulteration
Dr. Amy Bauer, TSI Incorporated
Olive oil is among the most commonly adulterated food products.  Raman spectroscopy has the potential to be utilized in measurements of olive oil to establish purity from adulteration with other, less expensive, oils. This application note reviews some of the most compelling data present in recent scientific literature to support this claim.
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Thin Film Analysis Using a UV-Vis Spectrophotometer and 5 Degree Relative Specular Reflectance Accessory
Shimadzu
Whether multiple or single anti-reflection (AR) coatings are applied to a substrate, it is of critical importance that the individual coatings be analyzed for film thickness prior to making a finished product. This note demonstrates measurement of a single protective coating on an acrylic substrate using UV-Vis with a 5 degree relative specular reflectance accessory and film thickness software.
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Two Excitation Wavelengths Are Better than One
Frederick G. Haibach, PhD, and Huawen Wu, PhD, BaySpec, Inc.
The ability to use two Raman excitation wavelengths in a single instrument improves both applicability and specificity on real-world samples. The gains are more than just a simple “sum of parts."
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