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February 2013
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Biopharm
Analyzing EPA 8270D with New Semi-Volatiles GC Column
Kory Kelly, Phenomenex
A GC–MS method analyzing base/neutral/acids (BNAs) is presented using the Zebron™ ZB-SemiVolatiles GC column.  Specific attention is paid to the behavior of typically poor performing compounds like pyridine and PCP.
 
Examining the Role of Inertness for Semi-Volatile Methods
Kory Kelly and Kristen Parnell, Phenomenex
Have you ever "primed" your column or used thicker films (≥ 0.50 µm) to overcome column activity?  This 3-min presentation examines the influence of Enviro-Inert™ Technology on active compound performance.
 
Improved PAH Recoveries with Simultaneous Humic Acids Removal
Zeshan Aqeel, Seyed Sadjadi, and Erica Pike, Phenomenex
Polycyclic aromatic hydrocarbons are effectively extracted from water samples (EPA Method 550.1) while humic acids, common chromatographic interferents, are removed from the sample using Strata® PAH soild phase extraction tubes.

Pharma
A Rapid and Reliable Method for Chlorinated Pesticides
Kory Kelly, Phenomenex
A rapid analysis of chlorinated pesticides (EPA Method 8081) is presented in under 10 min, delivering shorter cycle times and improved lab productivity.  Baseline separation of all analytes is achieved.
 
Increased Pesticide Recoveries with Automated Extraction from Water
Kali Tudela, Phenomenex and David Gallagher and Michael Ebitson, Horizon Technology, Inc.
A method using automated extraction followed by GC has been developed to improve throughput and recoveries of pesticides in EPA Method 508.1.
 
LC–MS-MS and GC–MS Analysis of Triazine Herbicides
Kory Kelly and Kali Tudela, Phenomenex
Two methods are presented for triazine herbicides analysis in drinking water (EPA Method 536) and wastewater (EPA Method 619) exhibiting resolution and sensitivity improvements as well as time savings.

Pharma
Leveraging High-Tempreature Gas Chromatography for DRO Analysis
Kali Tudela and Kory Kelly, Phenomenex
Considerations should be taken to ensure reproducible results over repeated injections of heavy compounds. This technical note discusses advantages of using a GC column stable to 430 °C when analyzing DROs.

Pharma
Improved Extraction and GC Analysis of Haloacetic Acids
Shahana Huq, Matthew Trass, and Erica Pike, Phenomenex
Haloacetic acids (EPA Method 552.1) are effectively extracted and concentrated from water using a high-capacity polymeric strong anion exchange SPE sorbent, providing benefits including dryout resistance and reduced solvent consumption.

Pharma
Give Your Lab the Environmental Edge
Phenomenex
As new regulations and updated methods arise, up-to-date technical information can help guide your lab's analyses. Find the latest environmental tips, articles, and product news in the "Environmental Edge" newsletter.
 
Environmental Monitoring and Testing Online Resources
Phenomenex
Access the latest online environmental applications, technical notes, new product releases, and more.